In 1998-99 a green
lab was offered as an alternative to the normal organic lab sequence
at the University of Oregon. This
two-term sequence, taught by Jim Hutchison
and Ken Doxsee consisted
of two sections with twelve students each. Additionally, three teaching
assistants, Marvin Warner, Scott Reed, and Brad Wan worked with the
students in the lab to optimize and test new green laboratory experiments.
For the 1999-00 year, the green lab was expanded
to a class of 30 students, to further test the experiments, conduct
monitoring of waste production and air monitoring. Today, all organic
labs are taught in the green format in our new green organic lab.
The goal in designing
this course was two-fold. We sought to teach students the core organic
synthesis laboratory skills while demonstrating, first hand, the benefits
of an approach that uses greener reagents, reaction conditions and products.
Our belief is that the introduction of greener experiments will improve
safety, allow for the routine use of macroscale techniques, and provide
an ideal context for the discussion of chemical safety.
One of the challenges
in developing this course was developing new laboratory experiments,
as there are very few examples in current lab manuals. Our criteria
for identifying green experiments for this new curriculum were that
each experiment:
- Illustrate green chemical
concepts (e.g. recycling, hazard reduction, solvent reduction)
- Teach modern reaction
chemistry and techniques
- Complement the lecture
course and provide a platform for discussion of environmental issues
in the classroom
- Be accomplished by students
given the time (3 hours) and material constraints of a typical student
organic laboratory
- Is adaptable to either
macroscale or microscale methods
- Uses inexpensive, greener
solvents and reagents
- Reduces laboratory waste
and hazards
- Each term of the lab course
consists of 7 labs that were either designed from scratch or modified
from existing labs to meet the above criteria.